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Crystallization of Indomethacin from the Amorphous State below and above Its Glass Transition Temperature

https://doi.org/10.1002/jps.2600831211
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What this work says

Outgoing claims: the papers this work cites, builds on, or argues with.

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Crystallization in polymers
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Sequences of precipitate nucleation
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The nucleation of metastable phases from undercooled liquids
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Kinetic aspects of the glass-transition behaviour of maltose—water mixtures
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Viscoelastic properties of polymers
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Structural instability and relaxation in liquid and glassy phases near the fragile liquid limit
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The molecular basis of moisture effects on the physical and chemical stability of drugs in the solid state
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Advances in Food and Nutrition Research
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Crystallization of Polymers
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Volumetric interpretation of viscosity for concentrated and dilute sugar solutions
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Sugar Crystallization, Equilibrium Moisture Content and Crystallization of Amorphous Sucrose and Glucose
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Non-Isothermal and Isothermal Crystallization of Sucrose from the Amorphous State
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Physical Properties of Aromatic Hydrocarbons. I. Viscous and Viscoelastic Behavior of 1:3:5-Tri-α-Naphthyl Benzene
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Rate of Nucleation in Condensed Systems
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Physical Properties of Aromatic Hydrocarbons. II. Solidification Behavior of 1,3,5-Tri-α-Naphthylbenzene
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Plasticizing Effect of Water on Thermal Behavior and Crystallization of Amorphous Food Models
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Viscoelastic Properties of Polymers
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Stability and several physical properties of amorphous and crystalline forms of indomethacin.
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Physicochemical characterization of indomethacin polymorphs and the transformation kinetics in ethanol.
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Some physicochemical properties of glassy indomethacin.
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A kinetic study of the crystallization process of noncrystalline indomethacin under isothermal conditions.
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Glassy state of pharmaceuticals. III. Thermal properties and stability of glassy pharmaceuticals and their binary glass systems.
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Glassy state of pharmaceuticals. IV. Studies on glassy pharmaceuticals by thermomechanical analysis.
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Use of Metastable Phase Diagrams in Rapid Solidification
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Strong and Fragile Behavior in Liquid Polymers

What points at this work

Incoming claims: where this work appears in other papers’ reference lists and arguments.

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Polymorphic Transformation of Indomethacin Under High Pressures**The previous affiliation when this study was done, Organic Synthesis Research Laboratory, Sumitomo Chemical Co., Ltd. 3-1-98, Kasugade-naka, Konohana-ku, Osaka 554-8558, Japan.
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Prediction of the Thermal Phase Diagram of Amorphous Solid Dispersions by Flory–Huggins Theory
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Inhibition of indomethacin crystallization in poly(vinylpyrrolidone) coprecipitates
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Effect of Polyvinyl Pyrrolidone on the Thermal Phase Transition of 1,2 Dipalmitoyl-sn-glycero-3-phosphocholine Bilayer
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Screening for differences in the amorphous state of indomethacin using multivariate visualization
inferred← citeshttps://doi.org/10.1016/j.ejps.2007.07.003openalex-snapshot
Quantifying ternary mixtures of different solid-state forms of indomethacin by Raman and near-infrared spectroscopy
inferred← citeshttps://doi.org/10.1016/j.ejps.2009.04.005openalex-snapshot
Correlating thermodynamic and kinetic parameters with amorphous stability
inferred← citeshttps://doi.org/10.1016/j.ejps.2009.06.007openalex-snapshot
Using the low-frequency Raman spectroscopy to analyze the crystallization of amorphous indomethacin
inferred← citeshttps://doi.org/10.1016/j.ejps.2009.09.009openalex-snapshot
Molecular mobility in liquid and glassy states of Telmisartan (TEL) studied by Broadband Dielectric Spectroscopy
inferred← citeshttps://doi.org/10.1016/j.ejps.2016.04.001openalex-snapshot
Solubility and dissolution enhancement of efavirenz hot melt extruded amorphous solid dispersions using combination of polymeric blends: A QbD approach
inferred← citeshttps://doi.org/10.1016/j.ejps.2018.04.030openalex-snapshot
Molecular dynamics, physical and thermal stability of neat amorphous amlodipine besylate and in binary mixture
inferred← citeshttps://doi.org/10.1016/j.ejps.2019.104955openalex-snapshot
Impact of phase separation morphology on release mechanism of amorphous solid dispersions
inferred← citeshttps://doi.org/10.1016/j.foodchem.2011.12.011openalex-snapshot
Molecular mobility in a homologous series of amorphous solid glucose oligomers
inferred← citeshttps://doi.org/10.1016/j.foodchem.2020.126884openalex-snapshot
Exploring the solid-state phases and thermodynamics of calcium l-lactate
inferred← citeshttps://doi.org/10.1016/j.foodres.2017.05.021openalex-snapshot
Amorphization of thiamine chloride hydrochloride: A study of the crystallization inhibitor properties of different polymers in thiamine chloride hydrochloride amorphous solid dispersions
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2004.01.038openalex-snapshot
Microscopic molecular mobility of amorphous AG-041R measured by solid-state 13C NMR
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2004.06.009openalex-snapshot
Stability study of amorphous valdecoxib
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2004.12.019openalex-snapshot
Solid dispersion particles of amorphous indomethacin with fine porous silica particles by using spray-drying method
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2005.08.021openalex-snapshot
Inhibition of a solid phase reaction among excipients that accelerates drug release from a solid dispersion with aging
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2006.11.064openalex-snapshot
Formulation, lyophilization and solid-state properties of a pegylated protein
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2007.05.046openalex-snapshot
Phase characterization of indomethacin in binary solid dispersions with PVP VA64 or Myrj 52
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2008.11.018openalex-snapshot
Enhancement of oral bioavailability of an HIV-attachment inhibitor by nanosizing and amorphous formulation approaches
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2009.06.029openalex-snapshot
Effect of wet milling process on the solid state of indomethacin and simvastatin
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2009.07.006openalex-snapshot
Monitoring crystallisation of drugs from fast-dissolving oral films with isothermal calorimetry
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2009.08.037openalex-snapshot
Prediction of recrystallization behavior of troglitazone/polyvinylpyrrolidone solid dispersion by solid-state NMR
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2009.09.035openalex-snapshot
An improved kinetics approach to describe the physical stability of amorphous solid dispersions
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2010.07.049openalex-snapshot
Application of Partial Least-Squares (PLS) modeling in quantifying drug crystallinity in amorphous solid dispersions
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2010.12.018openalex-snapshot
Assessment of crystalline disorder in cryo-milled samples of indomethacin using atomic pair-wise distribution functions
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2011.01.031openalex-snapshot
The contribution of Raman spectroscopy to the analysis of phase transformations in pharmaceutical compounds
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2011.06.050openalex-snapshot
Physicochemical stability of high indomethacin payload ordered mesoporous silica MCM-41 and SBA-15 microparticles
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2011.10.040openalex-snapshot
Tablet preformulations of indomethacin-loaded mesoporous silicon microparticles
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2011.10.055openalex-snapshot
An investigation into water interactions with amorphous and milled salbutamol sulphate: The development of predictive models for uptake and recrystallization
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2012.04.066openalex-snapshot
Emerging trends in the stabilization of amorphous drugs
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2013.12.025openalex-snapshot
Raman mapping for kinetic analysis of crystallization of amorphous drug based on distributional images
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2014.09.010openalex-snapshot
A comparison of the effect of temperature and moisture on the solid dispersions: Aging and crystallization
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2015.08.101openalex-snapshot
Physical stability of drugs after storage above and below the glass transition temperature: Relationship to glass-forming ability
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2015.10.042openalex-snapshot
Thermoanalytical and Fourier transform infrared spectral curve-fitting techniques used to investigate the amorphous indomethacin formation and its physical stability in Indomethacin-Soluplus ® solid dispersions
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2017.08.121openalex-snapshot
Moisture-induced phase separation and recrystallization in amorphous solid dispersions
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2017.09.047openalex-snapshot
Design and pharmaceutical applications of a low-flow-rate single-nozzle impactor
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2018.01.050openalex-snapshot
Impact of chirality on the Glass Forming Ability and the crystallization from the amorphous state of 5-ethyl-5-methylhydantoin, a chiral poor glass former
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2018.05.008openalex-snapshot
A comparative study between hot-melt extrusion and spray-drying for the manufacture of anti-hypertension compatible monolithic fixed-dose combination products
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2018.07.029openalex-snapshot
Predicting physical stability of ternary amorphous solid dispersions using specific mechanical energy in a hot melt extrusion process
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2019.118917openalex-snapshot
Impact of amorphization and GI physiology on supersaturation and precipitation of poorly soluble weakly basic drugs using a small-scale in vitro transfer model
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2020.119284openalex-snapshot
Tannic acid as a co-former in co-amorphous systems: Enhancing their physical stability, solubility and dissolution behavior
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2021.120883openalex-snapshot
Supersaturated formulations of poorly soluble weak acid drugs evaluated in rodents; a case study
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2023.122645openalex-snapshot
Poly (amino acid)s as new co-formers in amorphous solid dispersion
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2023.122840openalex-snapshot
Co-amorphous systems consisting of indomethacin and the chiral co-former tryptophan: Solid-state properties and molecular mobilities
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2024.124820openalex-snapshot
Mechanisms of dissolution and crystallization of amorphous glibenclamide
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2025.125331openalex-snapshot
Stability and recrystallization of amorphous solid dispersions prepared by hot-melt extrusion and spray drying
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2025.125441openalex-snapshot
A comprehensive overview of the role of intermolecular interactions in amorphous solid dispersions
inferred← citeshttps://doi.org/10.1016/j.ijpharm.2025.126245openalex-snapshot
Programmable delayed-release container system (PDRCS) for chronotherapeutic delivery: application in personalized treatment for Addison’s disease
inferred← citeshttps://doi.org/10.1016/j.ijpx.2020.100052openalex-snapshot
Physical stability and release properties of lumefantrine amorphous solid dispersion granules prepared by a simple solvent evaporation approach
inferred← citeshttps://doi.org/10.1016/j.ijpx.2021.100092openalex-snapshot
Formulating a heat- and shear-labile drug in an amorphous solid dispersion: Balancing drug degradation and crystallinity
inferred← citeshttps://doi.org/10.1016/j.jconrel.2017.11.005openalex-snapshot
Recent strategies in spray drying for the enhanced bioavailability of poorly water-soluble drugs
inferred← citeshttps://doi.org/10.1016/j.jddst.2019.01.017openalex-snapshot
Characterization of amorphous solid dispersions: An update
inferred← citeshttps://doi.org/10.1016/j.jddst.2019.101395openalex-snapshot
Stable amorphous solid dispersions of fenofibrate using hot melt extrusion technology: Effect of formulation and process parameters for a low glass transition temperature drug
inferred← citeshttps://doi.org/10.1016/j.jddst.2021.103065openalex-snapshot
Self-micellizing solid dispersion of atorvastatin with improved physicochemical stability and oral absorption
inferred← citeshttps://doi.org/10.1016/j.jddst.2023.104746openalex-snapshot
Development, recent advances, and updates in binary, ternary co-amorphous systems, and ternary solid dispersions
inferred← citeshttps://doi.org/10.1016/j.jfoodeng.2012.05.004openalex-snapshot
Impact of compression, physical aging, and freezing rate on the crystallization characteristics of an amorphous sugar matrix
inferred← citeshttps://doi.org/10.1016/j.jnoncrysol.2006.02.130openalex-snapshot
Transformations of glassy indomethacin induced by ball-milling
inferred← citeshttps://doi.org/10.1016/j.jnoncrysol.2014.08.055openalex-snapshot
The amorphous state of pharmaceuticals obtained or transformed by milling: Sub-Tg features and rejuvenation
inferred← citeshttps://doi.org/10.1016/j.jnoncrysol.2015.08.026openalex-snapshot
Fracture of molecular glasses under tension and increasing their fracture resistance with polymer additives
inferred← citeshttps://doi.org/10.1016/j.jpba.2017.12.001openalex-snapshot
Differential scanning calorimetry isothermal hold times can impact interpretations of drug-polymer dispersability in amorphous solid dispersions
inferred← citeshttps://doi.org/10.1016/j.molliq.2025.128981openalex-snapshot
Kinetics of melt and cold crystallization of antiferroelectric smectic phase
inferred← citeshttps://doi.org/10.1016/j.polymer.2024.126967openalex-snapshot
Cold crystallization of polytrimethylene terephthalate and copolymers
inferred← citeshttps://doi.org/10.1016/j.supflu.2015.08.023openalex-snapshot
Supercritical impregnation of polymer matrices spatially confined in microcontainers for oral drug delivery: Effect of temperature, pressure and time
inferred← citeshttps://doi.org/10.1016/j.supflu.2023.105990openalex-snapshot
Solubility of naproxen and indomethacin in supercritical carbon dioxide/ethyl acetate mixtures
inferred← citeshttps://doi.org/10.1016/j.trac.2018.08.013openalex-snapshot
Chemometrics coupled to vibrational spectroscopy and spectroscopic imaging for the analysis of solid-phase pharmaceutical products: A brief review on non-destructive analytical methods
inferred← citeshttps://doi.org/10.1016/j.trac.2022.116698openalex-snapshot
A review on multivariate curve resolution applied to spectroscopic and chromatographic data acquired during the real-time monitoring of evolving multi-component processes: From process analytical chemistry (PAC) to process analytical technology (PAT)
inferred← citeshttps://doi.org/10.1016/j.vibspec.2011.09.009openalex-snapshot
Measurement of amorphous indomethacin stability with NIR and Raman spectroscopy
inferred← citeshttps://doi.org/10.1016/j.xphs.2016.05.001openalex-snapshot
Interrelationships Between Structure and the Properties of Amorphous Solids of Pharmaceutical Interest
inferred← citeshttps://doi.org/10.1016/j.xphs.2016.07.001openalex-snapshot
Mannitol/ l -Arginine-Based Formulation Systems for Freeze Drying of Protein Pharmaceuticals: Effect of the l -Arginine Counter Ion and Formulation Composition on the Formulation Properties and the Physical State of Mannitol
inferred← citeshttps://doi.org/10.1016/j.xphs.2016.07.009openalex-snapshot
Co-amorphous Formation Induced by Combination of Tranilast and Diphenhydramine Hydrochloride
inferred← citeshttps://doi.org/10.1016/j.xphs.2016.08.019openalex-snapshot
The Slow Relaxation Dynamics in the Amorphous Pharmaceutical Drugs Cimetidine, Nizatidine, and Famotidine
inferred← citeshttps://doi.org/10.1016/j.xphs.2018.11.002openalex-snapshot
Fifty-Eight Years and Counting: High-Impact Publishing in Computational Pharmaceutical Sciences and Mechanism-Based Modeling
inferred← citeshttps://doi.org/10.1016/j.xphs.2019.10.054openalex-snapshot
Insight From Molecular Dynamics Simulations on the Crystallization Tendency of Indomethacin Polymorphs in the Undercooled Liquid State
inferred← citeshttps://doi.org/10.1016/j.xphs.2020.08.006openalex-snapshot
A Mechanistic Model for Predicting the Physical Stability of Amorphous Solid Dispersions
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