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Revealing the Role of CO during CO2 Hydrogenation on Cu Surfaces with In Situ Soft X-Ray Spectroscopy

https://doi.org/10.1021/jacs.2c12728
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What this work says

Outgoing claims: the papers this work cites, builds on, or argues with.

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Beyond Oil and Gas: The Methanol Economy
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Towards Oil Independence Through Renewable Methanol Chemistry
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Heterogeneous Catalysis of CO2 Conversion to Methanol on Copper Surfaces
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Advanced analysis of copper X‐ray photoelectron spectra
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Methanol Synthesis and Reverse Water–Gas Shift Kinetics over Cu(110) Model Catalysts: Structural Sensitivity
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Methanol Synthesis from CO2, CO, and H2over Cu(100) and Ni/Cu(100)
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Methanol synthesis on a Cu(100) catalyst
inferredcites →https://doi.org/10.1007/s10562-019-03036-7openalex-snapshot
Bifunctional Synergy in CO Hydrogenation to Methanol with Supported Cu
inferredcites →https://doi.org/10.1007/s11244-018-1075-2openalex-snapshot
2D Material Membranes for Operando Atmospheric Pressure Photoelectron Spectroscopy
inferredcites →https://doi.org/10.1016/0039-6028(92)90460-nopenalex-snapshot
Interactions of O2, CO, CO2, and D2 with the stepped CU(311) crystal face: Comparison to CU(110)
inferredcites →https://doi.org/10.1016/0039-6028(92)90579-uopenalex-snapshot
Surface hydride formation on a metal oxide surface: the interaction of atomic hydrogen with Cu2O(100)
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A study on CO2 dissociation on a stepped (332) copper surface
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Methanol Production and Applications: An Overview
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Systematic and collaborative approach to problem solving using X-ray photoelectron spectroscopy
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Ambient pressure X-ray photoelectron spectroscopy study of room-temperature oxygen adsorption on Cu(1 0 0) and Cu(1 1 1)
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CO2-based methanol and DME – Efficient technologies for industrial scale production
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Causation of catalytic activity of Cu-ZnO for CO2 hydrogenation to methanol
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Comparative study on the effect of different copper loading on catalytic behaviors and activity of Cu/ZnO/Al2O3 catalysts toward CO and CO2 hydrogenation
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Insight into methanol synthesis from CO2 hydrogenation on Cu(1 1 1): Complex reaction network and the effects of H2O
inferredcites →https://doi.org/10.1016/j.jcat.2020.11.035openalex-snapshot
The roles of CO and CO2 in high pressure methanol synthesis over Cu-based catalysts
inferredcites →https://doi.org/10.1016/j.physb.2009.05.058openalex-snapshot
Electronic structure of complex copper systems probed by resonant inelastic X-ray scattering at Cu edge
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Chemical kinetics of copper oxide reduction with carbon monoxide
inferredcites →https://doi.org/10.1016/j.rser.2015.01.010openalex-snapshot
Recent development in catalytic technologies for methanol synthesis from renewable sources: A critical review
inferredcites →https://doi.org/10.1016/s0039-6028(02)02550-5openalex-snapshot
Dissociative adsorption of hydrogen on strained Cu surfaces
inferredcites →https://doi.org/10.1016/s0166-9834(00)84123-8openalex-snapshot
Mechanism of methanol synthesis from CO2/CO/H2 mixtures over copper/zinc oxide/alumina catalysts: use of14C-labelled reactants
inferredcites →https://doi.org/10.1021/acs.jpcb.7b10732openalex-snapshot
Water Adsorption and Dissociation on Polycrystalline Copper Oxides: Effects of Environmental Contamination and Experimental Protocol
inferredcites →https://doi.org/10.1021/acs.jpcc.0c08262openalex-snapshot
Surface Orientation and Pressure Dependence of CO 2 Activation on Cu Surfaces
inferredcites →https://doi.org/10.1021/acs.jpcc.9b03888openalex-snapshot
Interaction of Atomic Hydrogen with the Cu2O(100) and (111) Surfaces
inferredcites →https://doi.org/10.1021/acs.jpclett.6b00640openalex-snapshot
Graphene Membranes for Atmospheric Pressure Photoelectron Spectroscopy
inferredcites →https://doi.org/10.1021/acs.jpclett.6b02273openalex-snapshot
Subsurface Oxygen in Oxide-Derived Copper Electrocatalysts for Carbon Dioxide Reduction
inferredcites →https://doi.org/10.1021/bk-2021-1396.ch008openalex-snapshot
Enclosed Cells for Extending Soft X-ray Spectroscopies to Atmospheric Pressures and Above
inferredcites →https://doi.org/10.1021/cs200055dopenalex-snapshot
Mechanism of Methanol Synthesis on Cu through CO 2 and CO Hydrogenation
inferredcites →https://doi.org/10.1021/ie901081fopenalex-snapshot
Modeling of the Kinetics for Methanol Synthesis using Cu/ZnO/Al 2 O 3 /ZrO 2 Catalyst: Influence of Carbon Dioxide during Hydrogenation
inferredcites →https://doi.org/10.1021/ja0301673openalex-snapshot
Reduction of CuO and Cu 2 O with H 2 : H Embedding and Kinetic Effects in the Formation of Suboxides
inferredcites →https://doi.org/10.1021/ja073727xopenalex-snapshot
Autocatalytic Water Dissociation on Cu(110) at Near Ambient Conditions
inferredcites →https://doi.org/10.1021/ja0768237openalex-snapshot
On the Mechanism of Low-Temperature Water Gas Shift Reaction on Copper
inferredcites →https://doi.org/10.1021/jacs.5b07451openalex-snapshot
Catalyst Chemical State during CO Oxidation Reaction on Cu(111) Studied with Ambient-Pressure X-ray Photoelectron Spectroscopy and Near Edge X-ray Adsorption Fine Structure Spectroscopy
inferredcites →https://doi.org/10.1021/jacs.6b04039openalex-snapshot
Dissociative Carbon Dioxide Adsorption and Morphological Changes on Cu(100) and Cu(111) at Ambient Pressures
inferredcites →https://doi.org/10.1021/jacs.8b07906openalex-snapshot
Steps Control the Dissociation of CO2 on Cu(100)
inferredcites →https://doi.org/10.1021/jp040080jopenalex-snapshot
Methanol Oxidation on a Copper Catalyst Investigated Using in Situ X-ray Photoelectron Spectroscopy
inferredcites →https://doi.org/10.1021/jp512831fopenalex-snapshot
Reaction of CO with Preadsorbed Oxygen on Low-Index Copper Surfaces: An Ambient Pressure X-ray Photoelectron Spectroscopy and Scanning Tunneling Microscopy Study
inferredcites →https://doi.org/10.1023/a:1012755616064openalex-snapshot
Determination of Site Specific Adsorption Energies of CO on Copper
inferredcites →https://doi.org/10.1023/a:1023555415577openalex-snapshot
Fundamentals of Methanol Synthesis and Decomposition
inferredcites →https://doi.org/10.1038/334577a0openalex-snapshot
Junction effect interactions in methanol synthesis catalysts
inferredcites →https://doi.org/10.1038/s41467-020-16342-1openalex-snapshot
The unique interplay between copper and zinc during catalytic carbon dioxide hydrogenation to methanol
inferredcites →https://doi.org/10.1038/s41467-021-21604-7openalex-snapshot
Operando high-pressure investigation of size-controlled CuZn catalysts for the methanol synthesis reaction
inferredcites →https://doi.org/10.1038/s41929-021-00625-xopenalex-snapshot
Following the structure of copper-zinc-alumina across the pressure gap in carbon dioxide hydrogenation
inferredcites →https://doi.org/10.1039/c001484bopenalex-snapshot
Fundamental studies of methanol synthesis from CO2 hydrogenation on Cu(111), Cu clusters, and Cu/ZnO(0001)
inferredcites →https://doi.org/10.1039/c3cp53991aopenalex-snapshot
Reduction mechanisms of the CuO(111) surface through surface oxygen vacancy formation and hydrogen adsorption
inferredcites →https://doi.org/10.1039/c4cs00122bopenalex-snapshot
Recycling of carbon dioxide to methanol and derived products – closing the loop
inferredcites →https://doi.org/10.1039/d0cp00347fopenalex-snapshot
Identifying the catalyst chemical state and adsorbed species during methanol conversion on copper using ambient pressure X-ray spectroscopies
inferredcites →https://doi.org/10.1039/d0dt00754dopenalex-snapshot
Mechanism of CO 2 conversion to methanol over Cu(110) and Cu(100) surfaces
inferredcites →https://doi.org/10.1063/1.4773583openalex-snapshot
Experimental and theoretical investigation of the electronic structure of Cu2O and CuO thin films on Cu(110) using x-ray photoelectron and absorption spectroscopy
inferredcites →https://doi.org/10.1063/1.4887362openalex-snapshot
Dissociative adsorption of CO2 on flat, stepped, and kinked Cu surfaces
inferredcites →https://doi.org/10.1073/pnas.1701405114openalex-snapshot
Subsurface oxide plays a critical role in CO 2 activation by Cu(111) surfaces to form chemisorbed CO 2 , the first step in reduction of CO 2
inferredcites →https://doi.org/10.1080/08940886.2022.2082181openalex-snapshot
The Versatile Soft X-Ray (VerSoX) Beamline at Diamond Light Source
inferredcites →https://doi.org/10.1088/0953-8984/1/sb/026openalex-snapshot
Does CO2dissociatively adsorb on Cu surfaces?
inferredcites →https://doi.org/10.1088/0953-8984/20/18/184025openalex-snapshot
In-situ X-ray photoelectron spectroscopy studies of water on metals and oxides at ambient conditions
inferredcites →https://doi.org/10.1103/physrevb.39.1541openalex-snapshot
Studies of copper valence states with Cu L3 x-ray-absorption spectroscopy
inferredcites →https://doi.org/10.1103/physrevb.45.3309openalex-snapshot
Unoccupied electronic structure and core-hole effects in the x-ray-absorption spectra of Cu2 O
inferredcites →https://doi.org/10.1103/physrevlett.86.460openalex-snapshot
Bridging the Pressure Gap in Surface Science at the Atomic Level: H / Cu ( 110 )
inferredcites →https://doi.org/10.1107/s0909049513003592openalex-snapshot
Electron yield soft X-ray photoabsorption spectroscopy under normal ambient-pressure conditions
inferredcites →https://doi.org/10.1107/s1600577520009157openalex-snapshot
Ambient-pressure endstation of the Versatile Soft X-ray (VerSoX) beamline at Diamond Light Source
inferredcites →https://doi.org/10.1116/1.5053761openalex-snapshot
Carbon dioxide gas, CO2(g), by near-ambient pressure XPS
inferredcites →https://doi.org/10.1116/1.578101openalex-snapshot
Carbon dioxide chemistry on Cu(100)
inferredcites →https://doi.org/10.1126/science.1219831openalex-snapshot
The Active Site of Methanol Synthesis over Cu/ZnO/Al 2 O 3 Industrial Catalysts
inferredcites →https://doi.org/10.1126/science.aad8868openalex-snapshot
Activation of Cu(111) surface by decomposition into nanoclusters driven by CO adsorption
inferredcites →https://doi.org/10.1126/science.abj7747openalex-snapshot
The state of zinc in methanol synthesis over a Zn/ZnO/Cu(211) model catalyst
inferredcites →https://doi.org/10.1149/ma2011-01/4/151openalex-snapshot
Beyond Oil and Gas: The Methanol Economy
inferredcites →https://doi.org/10.3389/fenrg.2020.545431openalex-snapshot
Improving the Cu/ZnO-Based Catalysts for Carbon Dioxide Hydrogenation to Methanol, and the Use of Methanol As a Renewable Energy Storage Media

What points at this work

Incoming claims: where this work appears in other papers’ reference lists and arguments.

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Selective Co2 Hydrogenation for Targeted High-Value Products Over Pt/Cd-Tio2
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Electrocatalytic Reduction of CO 2 to Ethylene: Catalyst Design and Synchrotron‐Based Characterizations
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Electrochemical Cell Designs for Efficient Carbon Dioxide Reduction and Water Electrolysis: Status and Perspectives
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Synergistically catalytic hydrogenation of CO 2 and CO to methanol over Ga 2 O 3 promoted Cu/ ZnO / Al 2 O 3
inferred← citeshttps://doi.org/10.1002/aic.70504openalex-snapshot
Dynamic carbon cycling enables near‐100% CO selective CO 2 hydrogenation on carrier‐free Cu catalyst
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S‐doped Ag–Sn Alloy Hollow Microbox for High‐Performance CO2 Electroreduction to Formate
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Strukturelle und chemische Dynamik von Cu/NiO/Cu(100)‐Oberflächen während der CO 2 ‐Hydrierung
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S‐doped Ag–Sn Alloy Hollow Microbox for High‐Performance CO 2 Electroreduction to Formate
inferred← citeshttps://doi.org/10.1002/anie.8933772openalex-snapshot
Structural and Chemical Dynamics of Cu/NiO/Cu(100) Surfaces During CO 2 Hydrogenation
inferred← citeshttps://doi.org/10.1002/cctc.202400239openalex-snapshot
In Situ Formation of Suspended Graphene Windows for Lab‐Based XPS in Liquid and Gas Environments
inferred← citeshttps://doi.org/10.1002/cctc.202401425openalex-snapshot
Reactants‐Driven Surface‐Active Sites on a Cu/CeO2 Catalyst for Methanol Synthesis from Syngas
inferred← citeshttps://doi.org/10.1002/cjce.25683openalex-snapshot
A catalytic sites contiguity study on atomically‐dispersed ZnO ‐Cu/ SiO 2 catalysts to improve methanol formation from CO 2 hydrogenation
inferred← citeshttps://doi.org/10.1002/cphc.202300543openalex-snapshot
Ambient Pressure X‐ray Photoelectron Spectroscopy Study of Oxidation Phase Transitions on Cu(111) and Cu(110)
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3D Cu Microbuds for Electrocatalytic CO Reduction Reaction
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CO2 conversion into fuels and value-added chemicals: from molten salt catalysts to metal–organic and covalent–organic frameworks
inferred← citeshttps://doi.org/10.1007/s44371-026-00630-8openalex-snapshot
Size and symmetry dependent CO2 activation on Tin [n = 4, 8, 13] cluster: an insight from first principle
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Study on the effects of Nd-doping on the performance of Cu-based CO2 hydrogenation catalysts with different oxide supports
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The origin of the mediocre methanol selectivity of Cu/ZnO-based catalysts for methanol synthesis from CO2 hydrogenation
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Unveiling a synergistic ZrO2-Ga2O3 promotion strategy for copper catalysts: Enhanced methanol synthesis from CO2 via improved hydrogenation of formate intermediate
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Perchlorate decomposition on rhodium nanoclusters supported on copper crystallite (RhxCu) electrode in an electrodialysis-assisted bipolar electro-reduction system (ED-ER)
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Sorption-enhanced intensified CO2 hydrogenation via reverse water–gas shift reaction: Kinetics and modelling
inferred← citeshttps://doi.org/10.1016/j.cej.2024.158610openalex-snapshot
Anchoring Cu on Zirconium-oxo nodes in a pore-confined metal-organic framework for CO2 hydrogenation to methanol
inferred← citeshttps://doi.org/10.1016/j.cej.2025.164589openalex-snapshot
Nitrogen-doped TiO2 for promoting CO2 activation towards methanol synthesis over Cu-based catalyst
inferred← citeshttps://doi.org/10.1016/j.cej.2026.175072openalex-snapshot
Electron buffering by carbon dots enhances H2 activation and selective aldehyde hydrogenation over Cu/Al2O3 catalysts
inferred← citeshttps://doi.org/10.1016/j.cej.2026.175500openalex-snapshot
Active sites in Cu-based catalysts for CO2 hydrogenation to methanol: Characteristics and design strategies
inferred← citeshttps://doi.org/10.1016/j.cej.2026.178617openalex-snapshot
Calcination-modulated Cu redistribution in CuZr catalysts governs downstream ethylene glycol hydrogenolysis in dimethyl oxalate-to-ethanol conversion
inferred← citeshttps://doi.org/10.1016/j.ces.2025.122236openalex-snapshot
Electron isolation effect of Ga induced asymmetric microenvironment of support surface of Cu/nGa-TA catalyst to establish electron-rich interface to boost CO2 hydrogenation to CH3OH
inferred← citeshttps://doi.org/10.1016/j.checat.2025.101421openalex-snapshot
Effect of dilute Rh on oxygen dissociation, spillover, and the oxidation of Cu across many orders of magnitude pressure
inferred← citeshttps://doi.org/10.1016/j.checat.2026.101896openalex-snapshot
Reaction-driven exsolution from spinel ferrites for CO2 hydrogenation to short-chain hydrocarbons
inferred← citeshttps://doi.org/10.1016/j.ijhydene.2025.152146openalex-snapshot
Stability of Cu-based catalysts for CO2 hydrogenation to methanol
inferred← citeshttps://doi.org/10.1016/j.ijhydene.2026.155836openalex-snapshot
Zr as a structural and electronic mediator in Cu-spinel catalysts: Strengthening MSI for CO2 hydrogenation to methanol
inferred← citeshttps://doi.org/10.1016/j.jcat.2026.116865openalex-snapshot
Interfacial engineering coupling with surface hydroxylation for boosting n-propanol synthesis from syngas over CuCo-based catalyst
inferred← citeshttps://doi.org/10.1016/j.jcis.2025.02.019openalex-snapshot
Copper nanoparticles supported on metal-organic framework with topological defects for CO2 hydrogenation to methanol
inferred← citeshttps://doi.org/10.1016/j.jcis.2026.140356openalex-snapshot
Steering carbon dioxide electroreduction toward formic acid by Sn-induced Cu0 stabilization and optimized *OCHO intermediate adsorption
inferred← citeshttps://doi.org/10.1016/j.jcou.2026.103379openalex-snapshot
Towards the effects of plasma-based CO2-dissociation and subsequent catalytic green methanol synthesis using gas mixtures of CO2 and CO
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Unlocking the mystery of pulse-enhanced CO2 electroreduction on copper in carbonate media
inferred← citeshttps://doi.org/10.1021/acs.chemrev.4c00282openalex-snapshot
Understanding and Tuning the Effects of H2O on Catalytic CO and CO2 Hydrogenation
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Developing a Hybrid Modeling Framework for Enhanced Prediction in Chemical Reaction Kinetics
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Boosting the Methanol Yield of CO2 Hydrogenation by Strengthening Carbon-Mediated Hydrogen Spillover of a Copper–Zinc-Alumina Catalyst
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Unveiling Double Layer Effects in Electrocatalytic CO2 Reduction
inferred← citeshttps://doi.org/10.1021/acs.jpcc.5c05955openalex-snapshot
In Situ Studies of Copper-Zirconia-Zinc Oxide Model Catalysts for CO 2 Hydrogenation
inferred← citeshttps://doi.org/10.1021/acs.jpcc.5c05986openalex-snapshot
Benchmarking DFT Accuracy in Predicting O 1s Binding Energies on Metals
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Modeling Microenvironmental Effects in Heterogeneous Catalysis
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Existence of the Coadsorbed Phase of the CO Intermediates under CO 2 Activation with Hydrogen on Ru(0001)
inferred← citeshttps://doi.org/10.1021/acs.jpclett.3c01478openalex-snapshot
Size-Dependent Reactivity of Con– (n = 5–25) Cluster Anions toward Carbon Dioxide
inferred← citeshttps://doi.org/10.1021/acs.jpclett.3c03611openalex-snapshot
Influence of Selective Carbon 1s Excitation on Auger–Meitner Decay in the ESCA Molecule
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CO 2 Hydrogenation on Pd(111): The Role of Subsurface Hydrogen and Surface Defects
inferred← citeshttps://doi.org/10.1021/acsanm.5c05779openalex-snapshot
Colloidal Control of the Cu–ZnO Interface for Catalytic CO 2 Hydrogenation to Methanol
inferred← citeshttps://doi.org/10.1021/acscatal.5c08414openalex-snapshot
Mn-Promoted Surface Modification of MgO in Cu-Based Catalysts Enhances the Low-Temperature Reverse Water–Gas Shift Reaction
inferred← citeshttps://doi.org/10.1021/acscatal.6c03318openalex-snapshot
Catalyst and Catalysis Co-Exploration in Methane Utilization
inferred← citeshttps://doi.org/10.1021/acscatal.6c04165openalex-snapshot
Cu-Dominated Hydrogen Supply Modulation for Enhanced CO2 Hydrogenation to Methanol over ZnZrO x Catalysts
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Harnessing Selectivity in CO2 Hydrogenation: Mechanistic Descriptors, Data-Driven Catalyst Design, and Sustainability Constraints
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Selecting Reaction Pathways of CO 2 Hydrogenation on Ni(111) by Kinetic Hindrance Associated with the Initial Surface Conditions in the Treatment of H 2 /CO 2 Mixed Gas, Studied by Ambient-Pressure X-ray Photoelectron Spectroscopy
inferred← citeshttps://doi.org/10.1021/jacs.4c05813openalex-snapshot
Visualizing Catalytic Dynamics of Single-Cu-Atom-Modified SnS2 in CO2 Electroreduction via Rapid Freeze-Quench Mössbauer Spectroscopy
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Visualizing the Hidden Atomic Pathways of Iron Oxidation
inferred← citeshttps://doi.org/10.1038/s41467-023-40361-3openalex-snapshot
Unraveling surface structures of gallium promoted transition metal catalysts in CO2 hydrogenation
inferred← citeshttps://doi.org/10.1038/s41586-025-09394-0openalex-snapshot
Atomic dynamics of gas-dependent oxide reducibility
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Unveiling active sites and the cooperative role of non-thermal plasma and copper–zinc catalysts in the hydrogenation of CO2 to methanol
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Controlling the composition and elemental distribution of bi- and multi-metallic nanocrystals via dropwise addition
inferred← citeshttps://doi.org/10.1039/d4ey00273copenalex-snapshot
Cu–ZnO nanoparticles encapsulated in ZSM-5 for selective conversion of carbon dioxide into oxygenates
inferred← citeshttps://doi.org/10.1039/d4qi00812jopenalex-snapshot
Enhanced photocatalytic CO 2 reduction to CH 4 via restorable surface plasmon and Pd n –W δ + synergetic sites
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Recycling of organic ligands and solvents for successive synthesis of Cu-based nanocrystals towards CO 2 hydrogenation
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Spillover hydrogen-driven CO 2 hydrogenation on a Pd/Cu(111) single atom alloy model catalyst at room temperature studied by ambient pressure X-ray photoelectron spectroscopy
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Modeling thermocatalytic systems for CO 2 hydrogenation to methanol
inferred← citeshttps://doi.org/10.1039/d5sc03726copenalex-snapshot
Multiscale modeling of gas adsorption and surface coverage in thermocatalytic systems
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Catalytic CO 2 hydrogenation toward net-zero fuels and chemicals
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Coverage-dependent activation of CO over Ni/Cu(100) single atom alloys (SAAs)
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An electrochemical flow cell for operando XPS and NEXAFS investigation of solid–liquid interfaces
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VerSoX B07-B: a high-throughput XPS and ambient pressure NEXAFS beamline at Diamond Light Source
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CO2 Hydrogenation on Pd/Cu Single Atom Alloy Catalysts : Synchrotron-radiation XPS and DFT Studies
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Steering CO2 electroreduction toward HCOOH by Sn-induced Cu0 stabilization and optimized *OCHO intermediate adsorption
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Direct Spectroscopic Comparison of CO Adsorption over CuOx Prepared In Situ
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Constructing Co Cluster Sites for Selective CO2 Hydrogenation via Phase Segregation from Co-Doped TiO2 Nanocrystals
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